Thermal characterization of non-functionalized low content graphene nanoplatelets (GNP) added nylon 66 polymer

Abd Manaf, Mohd Edeerozey and Shueb, Mohammed Iqbal and Mohamed, Mahathir and Umar, Khairil Nor Kamal and Mohamad, Noraiham and Abd Razak, Jeeferie and Abdullah Sani, Nurhernida (2022) Thermal characterization of non-functionalized low content graphene nanoplatelets (GNP) added nylon 66 polymer. Journal of Advanced Research in Fluid Mechanics and Thermal Sciences, 89 (1). pp. 13-25. ISSN 2289-7879

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Abstract

Thermal behaviour of graphene nanoplatelets (GNP) reinforced nylon 66 nanocomposites were investigated using differential calorimetric scanning (DSC), thermogravimetric analyzer (TGA) and dynamic mechanical analysis (DMA). The influence of low content GNP on thermal properties of GNP/nylon 66 nanocomposites was studied for low GNP content (0.3, 0.5 and 1.0 wt%). DSC results indicate that addition of GNP increases crystallization temperature and degree of crystallinity of the nanocomposites. Thermal stability and mass loss were studied through TGA analysis. The results show that thermal stability and weight loss of GNP/nylon 66 nanocomposites slightly improve with the GNP addition with an increase in the onset of degradation temperature as much as 10 °C. DMA analysis shows that GNP in the nylon 66 matrix act similar to plasticizer; it decreases the storage modulus and glass transition temperatures of the nanocomposites. GNP addition also reduces tan δ indicating an improvement in the damping property of the nanocomposites. Overall, this study concludes that a minimal amount of 0.3 wt% of GNP is effective in improving the thermal properties of nylon 66 composites.

Item Type: Article
Uncontrolled Keywords: Nylon 66, Graphene nanoplatelets, Nanocomposite, Thermal properties, DSC, TGA, DM
Divisions: Faculty of Manufacturing Engineering
Depositing User: mr eiisaa ahyead
Date Deposited: 14 Apr 2023 15:00
Last Modified: 14 Apr 2023 15:00
URI: http://eprints.utem.edu.my/id/eprint/26779
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